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GCMS comments for sample AD26478 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26478 revealed no non-target compounds.

NYC-WTC_000031739–000031761

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Oxirane, 2-methyl-3-propyl-, t Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.63 0.73 ng/uL 212237 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW Mol Form CAS# Qual

1 Oxirane, 2-methyl-3-propyl -, trans- 100 C6H120 006124-91-0 40 2 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H12O 006124-90-9 38 3 Heptane, 2,4-dimethyl- 128 C9H20 002213-23-2 23 4 Hexane, 2,3,4-trimethyl- 128 C9H20 000921-47-1 23 Abundance Scan 86 (5.627 min): 26478.D (-) m/z 41.10 100.00% 41

57 85 5000 71 -----------

5.20 5.40 5.60 5.80 6.00

mlz-? —PPP —4 20 30 40 .......... 11 50 60 70 80 ■ 1 i • • ■ 1 i ■ ■ ■ ■ i • • ■ ■ i ■ ■ ■ • i 1 ■ ■ ■ i • ■ 90 100 110 120 130 m/z 45.05 70.65% Abundance #1532: Oxirane, 2-methyl-3-propyl-, trans- 41

TAAT 11 44

C 5000 57 71 85 5.20 5.40 5.60 5.80 6.00 43.05 55.71% — 100 * ■ i * * * * । » , • , । i * » , j i । । i , . , । , ’11*111’1113 11 * • ■ • i miz-> 20 30 40I 50 60 70 80 90 110 100 120 130 Abundance #1531; Oxirane. 2-methyl-3-propyl-. cis- 43

57 5.20 5.40 15.60 5.80 6.00

N 5000 71 85 m/z 85.05 51.41%

100 1 ■ i ■ ■ 1 1 I ' 1 ' ' 1 1 ■ ■ i ■ • • 1 I 1 • 1 1 1 1 1 ‘ 1 I 1 1 1 1 1 1 1 1 1 1 1 1 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5145: Heptane, 2,4-dimethyl- i ■ • * ' i * • • i • ■ • • i ■ • ■ ■ i • ■ 43 5.20 5.40 5.60 5.80 6.00 m/z 57.10 49.35% 5000 85 27 57 71 —................ ----- m/z—> 20 30 40 50 60 70 --80--- 90 .... -28— 100 110 120 130 ■ TTfA I AAA - 5.20 5.40 5.60 5.80 6.00

26478.D NP112701.M Thu Dec 13 11:22:10 2001 Page 4

NYC-WTC_000031750

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