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GCMS analysis results for sample AD26320, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26320 with unidentified compounds detected.

NYC-WTC_000031319–000031332

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26320.D Vial: 19 Acq On 1 Dec 2001 4:35 am Operator: GALOS Sample gc/ms unknown 11/3 Inst GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.42 ng/uL 237140 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 23 2 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 23 3 Oxirane, 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 23 4 Hexane, 2-methyl- 100 C7H16 000591-76-4 17 Abundance Scan 597 (10.318 min): 26320.D (-) m/z 43.05 100.00% 43

5000 59 85 TTTTTTTfr 1tr’11’1 ’TI 73 10.00 10.20 10.40 10.60 38 + 1,..... TIM 100 ti 1111111 pTi rp 111111 n| 111 i 111111111 m/z 59.10 36.09% mlz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 110 115120 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

57 5000 71 85 10.00 10.20 10.40 10.60 m/z 57.10 34.71%

mlz-> .. ml — - mm -rrrrp-r 100 i ■ i ■•“ i" ■ •■ i.. 11.... ।.... |.... ।. 11' 1111' 111' 11' 11 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115120 Abundance #8516: Hexane, 1-propoxy- 43 4 Ar ■ r —A 10.00 10.20 10.40 10.60 5000 m/z 55.10 34.14% 56 85 I 61 73

miz-> ....... Mi ........ TT h - ।" i" " i 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 120 • i ■ ■ ■ ■ i ■ ■ ■ ‘r "

Abundance 43 #3003: Oxirane, 2,2-dimethyl-3-propyl- 59 85 । 1 I 1 1 1 1 I 1 ‘ 1 10.00 10.20 10,40 10.60 A_ m/z 41.05 31.51% 5000

72 — ...... .. |1.... ' I''''1'‘' 1 _ ... ............. 1''' ‘ 1"'11 ..... _...... 114 noag , . . L I''1111"111 '111111111" 1" T1111 “1'111'1111111111' 1111111 “ A AA m/z— > 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110115120 10.00 10.20 10.40 10.60

26320.D NP112701.M Tue Dec 04 10:13:05 2001 Page 3

NYC-WTC_000031329

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NYC-WTC_000031329Source: NYC Law Department, mirrored locally

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