GCMS analysis results sample AD26832, December 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26832.D Vial: 5 Acq On 6 Dec 2001 1:50 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Butanol, 3-methyl-, (S)- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.17 6.05 ng/uL 1742500 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 42 2 1,2-Pro' anediol, 3-methoxy- 106 C4H10O3 000623-39-2 36 3 2,3-But nediol 90 C4H10O2 000513-85-9 33 4 2-Butanol, 3-methyl-_________________ 88 C5H120 000598-75-4 9 Abundance • Scan 254 (7.175 min): 26832.D (-) m/z 45.05 100.00% 45

5000 61 73 —i । f । — 6.80 7.00 7.20 7.40 7.60

m/z-> mlll +788 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 i"" iH " r ■" r "11 207 i ‘111 r m/z 43 . 10 66.20% Abundance #852: 2-Butanol, 3-methyl-, (S)- i 415

5000 - ' । 1 1 1 1 । | TTr i । i i r i |" i 6.80 7.00 7.20 7.40 7.60

55 73 m/z 73.05 36.17% 27

miz-> + I 1 >. I” "I I"" I 1...... 87 I"1 ’ I' *' • I i" "i""i"■'r"'i• r■"i1"'i"1 ■ r1 ■' r'"r 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63660 1,2-Propanediol, 3-methoxy- 45

6.80 7.00 7.20 7.40 7.60 5000 - 75 m/z 61.10 35.99% 31 61 15 I 88 I'' ’ ’ I •'" I'1'' I 111111111 ■ * 11 ■■i> । T’T m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance #917:2,3-Butanediol 45 6.80 7.00 7.20 7.40 7.60 m/ z 44.05 13.48% 5000

29 19 1 — #4 11 r57 .1 75 90 ।■11 ■' , 1 [1"11"11111 *111"1 r1111" “ r11111" TTTT 11 n 111, । n 11111111111111 1 ■ ।" " । ■" ■ । ■ -A / m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 200 210 6.80 7.00 7.20 7.40 7.60

26832.D NP112701.M Fri Dec 07 14:55:41 2001 Page 8

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