GCMS analysis results sample AD26832, December 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC0601\26832.D Vial: 5 Acq On : 6 Dec 2001 1:50 pm Operator: GALOS Sample : gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Hexanol Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.46 ng/uL 133633 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 72 2 Amylene Hydrate 88 C5H120 000075-85-4 64 3 3-Hexanol 102 C6H140 000623-37-0 64 4 3-Hexanol 102 C6H140 000623-37-0 56 Abundance Scan 202 (6.698 min): 26832.D (-) m/ z 59.10 100.00% 59

5000 73 43 - -A4 6.40 6.60 6.80 7.00 -- Hr Tuat pTTTp-rTTp-rrrprrv^ I ■ ■ ■ ■ I ■ ■" I v m/ z 55.10) 84.22% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531: 3-Hexanol 59

5000 73 —,A—AA 6.40 6.60 6.80 7.00 43 m/z 73.05 41.30%

m/z-> TUTEpTTrm ITTIT + PTTTH ■ i>■■•।■ i ■ • i > > < < i * > > ■ i ■ • ■ • । ■ i ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62938; Amylene Hydrate 59 _____ / 1 ■ i ■ • • > i 6.40 6.60 6.80 7.00 73 5000 43 m/z 43.10 28.52% 31

26 11' ■ ■ i T‘T‘I"‘"11_ ____ ___ ‘1111111TETTTVEOTTCTVCOOUIEITETEOUET"TTICVCOOTTTTTETT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ... . “ #63529:3-Hexanol ” ‘ ... AA== -)? 59 6.40 6.60 6.80 7.00 m/z 41.05 . 05 20. J4e 20.64% 5000-

TI 31

44 73

102 mH +4 I " " i" ‘' r1 ’I—muIUOCTCTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 WNA6.40 6.60 6.80 7.00

26832.D NP112701.M Fri Dec 07 14:55:39 2001 Page 7

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