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GCMS analysis results for sample AD24293, Nov 7 2001

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Laboratory report documenting GCMS analysis of sample AD24293 conducted on November 7, 2001, noting unknown compounds.

NYC-WTC_000068198–000068212

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24292.D Vial: 11 Acq On : 1 Nov 2001 1:52 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.54 0.42 ug/1 58362 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentfative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 78 2 Amylene Hydrate 88 C5H12O 000075-85-4 39 3 DL-4,B/Octanediol 146 C8H18O2 022520-40-7 10 4 4-Heptanol 116 C7H16O 000589-55-9 9 Abundance “ Scan 163 (6.543 min: 24292.D (-) m/z 58.95 100.00% 55 53

5000 73

41 6.20 6.40 6.60 6.80 4; 85 . 1.. 1111... I. m/z 54.95 83.52% nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527:3-Hexanol 55^

5000 73 . . . I I . . . . yTKh p* 31 6.20 6.40 6.60 6.80 m/z 73.00 49.30%

TiZz-> Y 4+4 45 84 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 11.... I.... I.. 111..

Abundance #849: Amylene Hydrate

AA 55 6.20 6.40 6.60 6.80 5000 73 m/z 41.00 23.12% 31 27 42 45 70 + ■ I " "I' " ‘I I ‘ ' I' " I"... 1.... I. Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ^bundance #8867; DL-4,5-Octanediol ‘ I ■' ■' I ' ' ' ■ I ■ ‘ ' I 6.20 6.40 6.60 6.80 m/z 42.95 23.08% 73 50)0 43

■nfe-> 20 25 27

30 35 40 ' I'''' I ‘ ‘ 45 50 4^ 55 60 65 -r 70 ' I ' " ' I " " I ' ‘' 1 ‘ ' 75 80 85 90 AJ 6JP " 6.^ ' ‘ RSO' ' 6.80

24292.D NP103001.M Fri Nov 02 12:04:44 2001 Page 2

NYC-WTC_000068207

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NYC-WTC_000068207Source: NYC Law Department, mirrored locally

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