GC/MS analysis results for sample AD23271, Oct 15 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L * * * * * * *************************************************************** Peak Number 3 3-Hexanol Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.55 ug/1 55451 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hex^ol 102 C6H14O 000623-37-0 83 2 Amyle/e Hydrate 88 C5H12O 000075-85-4 39 3 3-Pe/tanol, 2-methyl- 102 C6H14O 000565-67-3 38 4 3-Heptanol 116 C7H16O 000589-82-2 36 Abundance/, Scan 172 (6.618 min): 23271.D (-) m/z 59.05 100.00% 5b-

253 73

41 — 6.20 6.40 6.60 6.80 7.00 ........ ” +4 I''........ I'H'i I'''' I " '' I' " ' I 100 "I""I "mT^ 55.00 88.22% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 '\bundance #63531:3-Hexanol 50

5000 73 ‘'i-rVI I I , I -I I ' ' ' ' I 6.20 6.40 6.60 6.80 7.00 43 m/T 73.00 45.23% A . ..... 11" " I" " I"'' I" " I" " I" "I TT/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62940: Amylene Hydrate 519 -

73 6.20 6.40 6.60 I6.80 '7.06' 5000 45 m/z 41.05 22.46% 31

" I" '' I'' t+t ■jn-n-p-initr ' I " " I" " I " '' I' " ' I" " I' ‘" I " " I' TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561: 3-Pentanol, 2-methyl- 5|9 6.20 6.40 6.60 6.80 7.00 mTz 43705 21.83% 5000 73

31 45 85 p-n-rp-m-r 4 I.... 11 rr ' I 102 I" " I " " I " " I " " I " " I " ‘' I' 6.20 6.40 6.60 6.80 ' 7.00 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110

23271.D NP091101.M Mon Oct 15 09:37:43 2001 Page 3

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