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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088272
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.44 ug/1 43429 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Hexan^ 102 C6H14O 000623-37-0 78 2 3-Pent^ol, 2-methyl- 102 C6H14O 000565-67-3 50 3 Amylene Hydrate 88 C5H12O 000075-85-4 42 4 2,3^utanediol, 2,3-dimethyl-_____ 118 C6H14O2 000076-09-5 40 Abundance Scan 172 (6.617 min): 23322.D (-) m/z 59.00 100.00% 5&

5000 73 41 . A. / 4^,.......... 6.20 6.40 6.60 6.80 7.00 , 1 53 . ........ 4+ U'l1 l'...... m/z 55.00 93.20% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ^bundance #63531:3-Hexanol 5)9

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z 73.00 46.48% "'I'.............. I............... .. ' I'" +4 I....... . Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561: 3-Pentanol, 2-methyl- 5(9 —I I I I I I I I I J| I Pl 1 I I I I 6.20 6,40 6,60 6.80 7.00 222 73 “m/z 41.05 27.89% 31 45 I'' “ I " '' I ^4^ 4 trrrrrr^ 85 102 ■ 11" • I" " I' ■" I" "I" " I" " I" " I' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62938; Amylene Hydrate 5^ 6.20 6.40 6.60 6.80 7.00 m/z 43.00 27.47% 73 5000 31 43

-rTTTTnjfl- 2e ....................... I............. ' I'''' I'''' I'''' I'' " I ‘ ' I'''' I' " ' I' ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

23322.D NP091101.M Mon Oct 15 10:25:52 2001 Page 3

NYC-WTC_00b'088272

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NYC-WTC_000088272Source: NYC Law Department, mirrored locally

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