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GCMS analysis results for sample AD24431, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.

NYC-WTC_000068413–000068431

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068423
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24431.D Vial: 11 Acq On : 3 Nov 2001 12:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.60 ug/1 82743 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-HexanoX 102 C6H14O 000623-37-0 72 2 3-Peii^^ol, 2-methyl- 102 C6H14O 000565-67-3 39 3 Amy>4ne Hydrate 88 C5H12O 000075-85-4 39 4 Octanal, 7-hydroxy-3,7-dimethyl- 172 C10H20O2 000107-75-5 36 (Kbundance Scan 164 (6.548 min): 24431 .D (-) m/z 59.05 100.00%

5000 73 43 ‘ ' I ' I ' ' ' ' p^' ' ' I ' 6.20 6.40 6.60 6.80

nfe-> ......... s llll|ii'ipbi|i) -rp- 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 84 100 TTp-rT+yTrrrjTTTT|TT^^ m/z 55.00 85.65% Abundance #63531:3-Hexanol 59

5000 73 ' I ’ ' ' ' I ' ' ' ' I ' ' ' ' I ' 6.20 6.40 6.60 6.80 43 m/z 73.00 45.28% TTTTyTTTTpTTTJTTTTy . .................. . +4 1........ . Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #1781: 3-Pentanol, 2-methyl- 5B

6.20 6.40 6.60 6.80 5000 31 73 m/z 42.95 29.34%

45 15 .... I..........I T I ” I ’t 4 J" " I 'I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #849: Amylene Hydrate $ 6.20 6.40 6.60 6.80 m/z 40.95 16.41%

5000 73 31

"‘'I""I""i'‘ 'I' ' r ' " I ' '"I " " I " I ' I " " I " " h' yTTTTjrrTTpTTTpTTTpTTTyr^^ •nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.20 6.40 6.60 6.80

24431.D NP103001.M Tue Nov 13 10:06:20 2001 Page 3

NYC-WTC_000068423

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NYC-WTC_000068423Source: NYC Law Department, mirrored locally

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