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GCMS analysis results, sample AD23844, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23844 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067439–000067452

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067449
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23844.D Vial: 4 Acq On : 17 Oct 2001 4:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.61 ug/1 57350 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanoy 102 C6H14O 000623-37-0 83 2 Amylene ^Hydrate 88 C5H120 000075-85-4 40 3 3-Pentyiol 88 C5H12O 000584-02-1 36 4 Silane/ trimethyl- 74 C3H10Si 000993-07-7 33 Wjuncteince Scan 172 (6.617 min): 23844.D (-) m/z 59.05 100.00% 55 50

5000

TiZz-> ^buncfeince 20 25 30 35 40 43

45 50 4+4 55 60 65 73

I . >I■‘111.... I > 1.11.... I.... I" 70 75 80 85 90 95 6.20 m/^ JL ^40 ' ‘ ROT “ 6.ro “ 7.00' 55.00 85.16% #63528:3-Hexanol 50 55

73 5000 31 6.20 6,40 6.60 6.80 7.00 m/z 73.00 51.34%

TlZz-> 20 .1,1... 25 30 35 40 4+4 45 50 55 60 65 70 84 75"m"m"m"^ Abundance #849: Amylene Hydrate

55 6.20 6.40 6.K) 6.80 7.00 5000- 73 m/z 43.05 26.59% 31 27 42 45 70 ............ ‘ ‘ I"" I'"' h'' I' ’ I' “ ‘ I ‘ ' I ‘ “ I' nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62942:3-Pentanol 50 6.20 6.40 6.60 6.80 7.00 m/z 41.00 22.57% 31 5000 41 27

■nfe-> 20 X 25 30 35 40 45 a) 55 ■ I'''' I' 60 65 87 6.20 6.40 6.60 6.80 7.00

23844.D NP101901.M Tue Oct 23 12:45:04 2001 Page 3

NYC-WTC_000067449

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NYC-WTC_000067449Source: NYC Law Department, mirrored locally

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