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GC/MS analysis results for sample AD22774, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22774 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087433–000087446

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087443
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22774.D Vial: 21 Acq On : 29 Sep 2001 8:03 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.46 ug/1 52965 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-Hex^ol 102 C6H14O 000623-37-0 83 2 3-Pen/anol 88 C5H12O 000584-02-1 50 3 Amylene Hydrate 88 C5H12O 000075-85-4 39 4 3-Pentanol, 2-methyl-____________ 102 C6H14O 000565-67-3 39 Abundance / Scan 172 (6.621 min): 22774.D (-) m/z 59705 100.00% f 5b 55

73 5000 41 14 6.20 6.40 6.60 6.80 7.00 ' I ’''' I' ‘' r ''' I' I I UiJ-TTITI I I / I +4 ' I'''' I'''' I' " ' I'''' I' m/z 55.00 70.04% ■nZz-> 20 25 30 35 40 45 50 55 60 75 80 85 90 95 Abundance #63528: 3-Hexanol

55

73 5000 -r-p-r-n-i-, , , , । 31 6.20 6.40 6.60 6.80 7.00 m/z 73/00 49.65% 27 45 84 ' I'''' I' ’' * I' ... ■ 11' ■' I' I 11'''' I ’' ’ ’ I''' ’ I " '' I' ii/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62941:3-Penlanol 5^

31 6.20 6.40 6.60 6.80 7.00 5000- m/z41700 25.28% 41 27 45 55 , 87 t+^ VHttV . 11... I.... I.... 1.11.11 ' I'''' I'''' I' ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #849; Amylene Hydrate 6.20 6.40 6.60 6.80 7.00 m/z 42795 22.17% 55 5000 73 31 27 42 45 70 ' I'''' I' . ................................ ' I'''' r ''' I'' '' I' Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6,20 6,40 6,60 6.80 7.00

22774.D NP091101.M Fri Oct 05 10:19:53 2001 Page 3

NYC-WTC_000087443

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NYC-WTC_000087443Source: NYC Law Department, mirrored locally

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