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GC/MS analysis results for sample AD22774, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22774 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087433–000087446

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087442
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22774.D Vial; 21 Acq On : 29 Sep 2001 8:03 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.01 ug/1 115671 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 X Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Methyl/ Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 PropaAal 58 C3H6O 000123-38-6 43 Abundance / Scan 157 (6.483 min): 22774.D (-) in/z 4^795 100.00% 4|3

58 5000

TTfe-> .... 20 30 Jll' 5050 160 40 5^7 4° 70 80 90 100 110 120 130 140 m/z 6.20 6.40 58.05 6.60 6.80 58.51% ^bundance #63387: 2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 100 “mTz 41.00 15.93% 71 85 I I I ' I ' ' ' ’ I ' ' ' ‘ I ' ' ' ' I ' Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 '\bundance ;#11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 _e2o__a4g_6w_6jo__ 5000 29 m/z 56.95 15.79%

' I ' ' ' ' I ' ' ' ' I I ,1 r-p-r^r*- 140 n&-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63351: Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6.80 m/z 100.00 12.89% 5000 58 27 I 85 100 1 I I I 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22774.D NP091101.M Fri Oct 05 10:19:51 2001 Page 2

NYC-WTC_000087442

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NYC-WTC_000087442Source: NYC Law Department, mirrored locally

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