GCMS analysis results for sample AD25733, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV1601\25733.D vial; 15 Acq On : 17 Nov 2001 4:41 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.42 0.41 ug/1 75755 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 3 Methyl ^obutyl Ketone 100 C6H12O 000108-10-1 58 4 Propanol 58 C3H6O 000123-38-6 43 Abundance Scan 150 (6.424 min); 25733. D (-) in/z 43.05 100.00% 43

5000

Tl/z-> 30 36 I. , ' i ' ' ' ' p ' p l 20 40 50 58

60 70 71

80 85

90 100 100

110 120 ......... 130 140 6.00 m/z 6.20 58.05 L 6.40 6.60 6.80 63.34% Abundance #63387: 2-Hexanone 43 58 5000

100 “Wz 41.00 .22.06% 71 85 I I I I I ■ I I ■ p I ■ I'l I I p ’ I ' I I ' ' p ' '' I I ' Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 40 58 6.00 6.20 6,40 6.60 6.80 5000 29 m/z SYTOO 21.09%

' I ' '‘ ' I ''''I I J. 71 I 85 100 140 ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63350; Methyl Isobutyl Ketone 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 13777%

5000 58

I 85 100 27 _ L 67 I ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ 1 ‘ ‘ ' I ' Tl^-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

25733.D GCMS1126.M Wed Nov 28 15:41:30 2001 Page 1

NYC-WTC_000069882