GCMS analysis results for sample AD25733, Nov 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25733.D Vial: 15 Acq On : 17 Nov 2001 4:41 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.41 ug/1 75755 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm / CAS# Qual 1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 2-HexanoiXe, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 3 Methyl ^obutyl Ketone 100 C6H12O 000108-10-1 58 4 Propanol 58 C3H6O 000123-38-6 43 Abundance Scan 150 (6.424 min): 25733.D (-) m/z 43705 100.00%!

58 5000

6.6o‘ 6.^ 'e.^' rot' 6.^ 36| I I ■ I . .-I ■ H 51 , V T T ' I' ■'' I ■ ‘ ‘' I' ‘' I ■'' ‘ I' ■ ■ ■ I' •'' I' ■ ■ • I' m/z 58.05 63.34% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63387:2-Hexanone 43

58 5000 6.00 ' R^ ' R^ ' ' ROT ‘ ROT '

100 "mTz 41.00 -22.06% 71 85 ■ I < i • 1 • • • "'l I ’ I'' ■ ‘ I' mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 eno 6.^' 6,^' 'rot' 'rot' 5000 29 m/z “57700 21.09%

7,1 85 100 ' I' ‘ ‘' 1 • > • ■ 11 ■ •. (. Wn*— -■ I jy,, I........... [...If? mZz-> 20 30 40 50 60 70 80 9b"'i66"iw"i»"iM"i46 Abundance #63350: Methyl Isobutyl Ketone 43 6.00 6.20 6.40 m/z 100.05 13.77% 5000 58

85 100 . 67 I fn-p ’ 1 ‘ ’ I ' ' ‘ ‘ I ' ’ ' m/z-> 20 30 40 50 60 70 80 OT1001101M130140 6.00 6.^ 6.40 6.^ 6.M

25733.D GCMS1126.M Wed Nov 28 15:41:30 2001 Page 1

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