GCMS analysis results for sample AD25733, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25733.D Vial: 15 Acq On : 17 Nov 2001 4:41 am Operator: 209 GALOS Sanqple : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. ----------------- ________ 7.68 2.11 ug/1 393917 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 Acetone 58 C3H6O 000067-64-1 10 3 MorphoL(£ne, 4 -methyl - 101 C5H11NO 000109-02-4 9 4 5-HexeZ -2-one 98 C6H10O 000109-49-9 9 Abundance Scan 287 (7.681 min): 25733.D (-) ra/z42.9 5 100.00s 4(3

5000 59

101 7.40 7.60 7.80 8.00 ' ‘ I ' ' 1 ' ‘ ‘ 1 ' ' ' ' I ' ' ' ‘ I' ' ' ' I m/z 59.05 48.82% •nfe-> 10 20 30 40 50 a) 70 TO 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000- 59 7.40 7.60 7.80 8.00 m/z 101.05 20.67% 101

_L _ 27 83 ........................ I I '1^ nfe-> 10 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 43

7.40 ‘ 7.^' '/.to' 'ao6‘ 5000 m/z 58.05^18.04% 58 27 + I ' ' ' ' 1 ' ' ■ ■ I • ‘ ‘ ' I ' ' ■ ■ I ' ' ' ' I nyz-> 10 20 30 40 50 60 70 TO 90 100 110 Abundance #1640: Morpholine, 4-methyl- 43 ' '7.46 7.60 7.80 8.00 m/z 41.00 7.72% 5000 101 15 71 . 56 I ' I ' ( ' ■ I ' ' ' ' I ' ' ' I I ' ■ I ■ ■ ■ ■ I ‘ ■ I ■ ‘ ' I ‘ I ■ • ■ ' I ‘ ' I ' ■nfe-> 10 20 30 40 50 60 70 TO 90 100 110

25733.D GCMS1126.M Wed Nov 28 15:41:32 2001 Page 2

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