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GCMS analysis results for sample AD25264, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25264 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069530–000069539

Folder label: “GCMS Scan X 10/24/01 An 11/9/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\25259.D Vial: 8 Acq On : 9 Nov 2001 7:16 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.51 ug/1 442986 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4^ydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetone / 58 C3H6O 000067-64-1 10 3 Morpholine, A.- methyl - 101 C5H11NO 000109-02-4 9 4 Butane, 1-^hoxy-_______________ 102 C6H14O 000628-81-9 9 Abundance / Scan 288 (7.690 tnin): 25259.D (-) m/z 42T95 100.00% 4(3

59 5000

101 '7.^' 7.60' '7.80' 8.00'' .,....,^11 51 . tyrn-T 69 83 ■ ■ I ‘ ' I ' ‘ ‘ ‘ I ' ' ' ' I ■ ‘ ‘ Ip ■ ' ■ I ' m/z 59.05 52.46% nfe-> 10 20 30 40 50 60 70 80 90 100 110 \bundance #64275:2-Pentanone, 4-hyclroxy-4-methyl- 4^

5000 '7.^' 7.60 '7.80' 8.00' ' 59 m/z 101.05 2^/79% 15 31 101 I l I r-r-r^

5. n&-> ’ '1'0' '2b’ ’30 40 50 60 70 80 90 100 110 Abundance #62326: Acetone 40 7.40 7.60 7.80 8,00 5000 m/z 58.05 18.25% 58

27 « I • • I • ■ • I’l • • • ■ I I nfe-> 10 X 30 40 50 60 70 'sb' " m' " 106 ” iw ^bundance #1640: Morpholine, 4-methyi- 4i3 "7.^' ‘zro 7.m' 8.06 m/z 41.00 7.03% 5000 101 15 71

10 I ‘ I ' I ' 20 27

40 56 I ' I ' ' I ' 1 ' ‘ ‘ ' I ‘ ‘ ‘ ‘ I ' ' ' ' I ‘ 50 60 70 80 90 ' I ' ' ' ' I ' 100 110 ' '7.^ •nfe-> 30 7.60 7.80 8.00

25259.D NP103001.M Wed Nov 28 11:53:44 2001 Page 1

NYC-WTC_000069538

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NYC-WTC_000069538Source: NYC Law Department, mirrored locally

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