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GCMS analysis results for sample AD24695, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24695 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068708–000068719

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068717
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0501\24695.D Vial: 4 Acq On : 5 Nov 2001 2:11 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.11 ug/1 183085 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone', 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 45 2 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Acetoja:^ 58 C3H6O 000067-64-1 9 4 5-^exen-2-one 98 C6H10O 000109-49-9 9 ^bundarj^ ~~ Scan 289 (7.699 min): 24695.D (-) m/z 42.95 100.00% 4(3

59 5000

101 TTT

83 7.40 7.60 7.80 8.00 30 I mTz 59.05 51.60% ' I ' ' ' ' I ''' ' ' I ' ' ‘ I I ' ' ' ' I ' ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 —T— 7.40 7.60 7.80 8.00 m/z 101.05 21.91% 31 , I 11'''' 11''' I'''' I'''' I'''' I' iiZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4|3 I ■ 11111111 111.1 7,40 7.60 7.80 8.00 5000 m/z 58.05 17.72% 101 71 ' ' Ji ' ' ' I ' ' ' ' I ' 1 ' ' I ' ' ' ' I ' ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone ........... 40 7.40 7.60 7.80 8.00 m/z 41.05 6.28% 5000 58 27 .... ' I ' ' ' ' I ' ' ' ' I '' ' ' I '' ' ' I ' ' ' ' I ' 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24695.D NP103001.M Fri Nov 09 12:17:36 2001 Page 2

NYC-WTC_000068717

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NYC-WTC_000068717Source: NYC Law Department, mirrored locally

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