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GCMS analysis results for sample AD24950, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24950 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069128–000069138

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24950 .D Vial: 18 Acq On : 7 Nov 2001 5:20 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.05 ug/1 384229 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetone/ 58 C3H6O 000067-64-1 9 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydnoxy-2-pentanone______________ 102 C5H10O2 003142-66-3 9 Abundance A Scan 288 (7,685 tnin): 24950.D (-) ra/z 42795 100.00% 43

5000 59

101 '7.46' '7.^ zto' 8.60 ,f 83 207 Ihnrn* mTz 59.0s 49.50% mfe-> 10 20 30 40 50 60 70 80 90 1(K)110120130140150160170180190200210 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 m/z 101.05 21.39% 27 I Qo 101 I I v mZz-> 10 Z) 30 40 50 a) 70 80 90 100110120130140150160170180190200210 Abundance #62322: Acetone 43

7.40 7.60 7.80 8.00 5000- m/z 58.05 18.92% 58 27 J1. 11JI I’l I'j. t. /['11111111 -J- I IKI I ll>l| ll>l| II ll|l I ll|

nnfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1640: Morpholine. 4-methyl- 4t3 7.40 7.60 7.80 8.00 ra/z 41.05 7.16% 5000 101 71

mfe-> XX IxX I" " I "■'T 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 ]llll|ll<l|lll.|llll|llll| T -vAzW

7.40 7.60 7.80 8.00

24950.D NP103001.M Fri Nov 16 15:31:01 2001 Page 1

NYC-WTC_000069136

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NYC-WTC_000069136Source: NYC Law Department, mirrored locally

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