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GCMS analysis results for sample AD24216, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24216 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000067990–000068002

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24215.D Vial: 2 Acq On : 1 Nov 2001 4:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table LibraiTf : C:\DAT7kBASE\NBS75K.L

Peak Number ,2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.28 ug/1 259950 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 33 2 Morpholirfe, 4-methyl- 101 C5H11NO 000109-02-4 9 3 3-Hydro -2-pentanone 102 C5H10O2 003142-66-3 9 4 Butane/ 58 C4H10 000106-97-8 9 Abundance / Scan 288 (7.685 min): 24215.D (-) m/z 42.95 100.00% 4(3

5000

■nZz-> ’ ’I 10 ................ ' I ' ‘ 20 3?,I, ■ I ' ' ' ' I' 30 40 50 60 59

70 ra 80 ____ ra ' 1 ' r-n-p-h- 90 101

- -t-r-r 10) 110 m/z 7.40 JL 7.60 59.05 7.80 8.00 52779% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4b

5000 ‘7.^’ ‘7.^ '7.^ 8,00 59 m/z 100.95 23.45% 101

L 27 1 I 83 I I ■ • ' ' I ■ ■ ‘ ■ I •’• • • I ■ ■ J" " I' TTfe-> 10 20 30 40 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyI- 4t3 ----- i-i-rT-i-rT-i-i-rS-TrT-pFM*TY-r^^ 7.40 7.60 7.80 800 5000 m/z 58.05 16.61% 101 71 I 56 I ' ' |->-r+ I I' ■’“n TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 ' ’7.46 7.60 7.80 8.00 m/z 41.05 7.79% 5000 45 15 ..I...... II..... I ' ‘ ‘ ' I ‘ ‘ “ I ‘ ‘ ' I r-p I. 66 73 84 102 ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24215.D NP103001.M Tue Nov 06 11:44:41 2001 Page 2

NYC-WTC_000067999

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NYC-WTC_000067999Source: NYC Law Department, mirrored locally

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