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GCMS analysis results for sample AD24216, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24216 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000067990–000068002

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV0101\24215.D Vial: 2 Acq On : 1 Nov 2001 4:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.48 ug/1 98580 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForra CAS# Qual 1 2-Hexi .one 100 C6H12O 000591-78-6 91 2 2-He: .none, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 78 3 Met: ^1 Isobutyl Ketone 100 C6H12O 000108-10-1 50 4 2- ixanone, 4-hydroxy-3 -propy1- 158 C9H18O2 062338-17-4 39 (\bunda^ Scan 150 (6.419 min): 24215.D (-) m/z42.95 100.00% 40

58 5000

6.00 6.20 6.40 6.60 6.80 ............. .ail, TTTTTTrft^TTpTTTp-rrTjTT-nyrTTTyrr^^ m/z 58.05 53.88% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63387:2-Hexanon8 43

58 5000 -r|-,-,O.'| ■ ■ ■ ■ I , , ?-rp , 6.00 6.20 6.40 6.60 6.80 100 m/^ 57.00 13.91% 71 » I' ’«’ j' * • * 1 M +r I"" ■'-r HfiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 40 600 6.20 6.40 6.60 6.80 5000 “m/z 41.05 12.64% 58 27 100 ttt++t TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63354: Methyl Isobutyl Ketone 40 6.00 6.20 6.40 6.60 6.80 m/z 100.00 11.38% 5000 58 A \ 85 100 67 TTpTTT^TTTTpTTTyTrrrlr^^

■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.t)0 ' 6.20 6.40 6.60 6.80

24215.D NP103001.M Tue Nov 06 11:44:39 2001 Page 1

NYC-WTC_000067998

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NYC-WTC_000067998Source: NYC Law Department, mirrored locally

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