GC/MS analysis report for sample AD22545, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22545.D Vial: 11 Acq On : 26 Sep 2001 12:15 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.50 0.54 ug/1 65967 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hex, one 100 G6H12O 000591-78-6 91 2 2-He: none, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Oxi ne, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 4 Me .yl Isobutyl Ketone___________ 100 C6H12O 000108-10-1 53 4bundai Scan 159 (6.498 min): 22545.D (-) m/z 4^/95 100.00% 43

58 5000

. y71 ..85I,. ,|100,.. .... m/z 6.20 6.40 58.00 6.60 6.80 58.33% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ^bundance #1556; 2-Hexanone 43

58 5000 I . I I , , I i'] .'i . I I , I , ,''f , . 1 , 6.20 6.40 6.60 6.80 m/z 57.00 15767% 27 I J ■Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 41.05 13.50%

Ti/z-> 20 ' I' ‘H ''' I' ' ' I ' 30 40 50 .1. 71 85 100 I |l| , I , , i"i I I I I I I I , , , I I I I I I , , , , I ,

60 70^80^ 90 100 110 120 130 140 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 6.20 6.40 6.60 6.80 58 m/z 100.00 10.80% 5000 7r

7i/z~> 30 ' I ' ' ' ' I ' ' ' ' 1 ' 20 30 40 50 ■ 60 ,.,l, 70 85 I . ,1, 80 90 100 I 100 110 120 130 140 A 6.20 Mh 6.40 6.60 6.80

22545.D NP091101.M Wed Oct 03 15:09:29 2001 Page 2

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