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GCMS analysis results for sample AD24050, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24050 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067867–000067879

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24050.D Vial: 11 Acq On : 25 Oct 2001 10:27 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.46 0.78 ug/1 141207 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H12O 000591-78-6 87 2 2-Hexaarone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 3 Oxiri .e, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 4 Meth 1 Isobutyl Ketone__________ 100 C6H12O 000108-10-1 52 ^bundanc^ Scan 154 (6.456 min): 24050.D (-) m/z 42.95 100.00% 43

58 5000

T 71 100 6.20 6.40 6.60 6.80 ,1,... p 11,.......... I'.,, , I ■ , ,, I ■,,, I............ m/z 58.05 53.00% TTfe-> 20 30 40 50 60 70 80 90 100 110 120 1^ 14K) Abundance #1556:2-Hexanone 43

58 5000 ,,, I,,,, I,. ■ 6.20 6.40 6.60 6.80 m/z 57700 16.65% 27 ' I ' ' I ' ‘ ' , .II,, <1 7 TiZz-> 20 30 40 50 60 70 80 90 100 110 1g) 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl-

58 6.2) 6.40 6.60 6.80 5000 29 “m/z 41.05 16.22%

100 ' I' ‘'' I' I ■' 11 I 140 ' I ’' ‘ ’ I ' ' '' I ' ' ' ' I' m/z-> 20 30 40 50 60 70 80 90 100tl01^'"'l30140 Abundance #1530: Oxirane. 2-methyi-2-(1-inethylethyl)- 43 6.20 6.40 6.60 6.80 58 m/z 100.00 11.08% 5000 71 30 I I . . I 1 1 . . 1 . I 1 ’ ' I ■ ' ■ ■ I ' ' ' ‘ I ■ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.40 6.60 6.80

24050.D NP101901.M Fri Oct 26 10:25:59 2001 Page 1

NYC-WTC_000067875

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NYC-WTC_000067875Source: NYC Law Department, mirrored locally

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