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GCMS analysis results for sample AD24050, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24050 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067867–000067879

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24050.D Vial: 11 Acq On : 25 Oct 2001 10:27 pm Operator: 209 G2VLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.69 0.47 ug/1 85514 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan^ 102 C6H140 000626-93-7 83 2 2-Pent^ol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Hex^ol, (S)- 102 C6H14O 052019-78-0 64 4 2-HeXanol, (R)- 102 C6H140 026549-24-6 43 Abundance Scan 180 (6.694 min): 24050.D (-) m/z 44.95 100.00% 4b5 :......... 5000

41 69 6.^ 51 I 8487 6.60 6.80 7.00 > ■' > I > ■' IP'" I ‘" I ‘' ■ h " “ I" " I • ’' h ‘ I “ I" “ I ‘ m/z 69.00 16.25% Tife-> 10 15 20 25 30 35 40 45a)55 60 65 70 75 80 85 90 95 Abundance #1792:2-Hexanol 4b

A[ I I I I j 5000 6.40 ‘6.60' aso' '7.60 m/z .41-05 14.93% ^5® ? 8487 • 1111.1,1.1111.... I.... 111111■I..1. .1111 Tlfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Sundance #63547:2-Pentanol, 4-melhyl- 4b 6,40 6.60 6.80 ' 7.66" ‘ 5000 m/z 44.00 11.00%

T 38 4^ 69 I 8487 ... 111.. 1.... I... 11....,.... I... 11.1.11.... I. nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769:2-Hexanol. (S)- 4b 6.40 6.60 6.80 7.00 m/z 42.95 10.71% 5000

..... ”........ 55 ? 8487 ' ‘ I''' ‘ I ‘' 1' ‘ ‘' I'''' I'''' I'''' I'" ’ I ‘' I' ‘' I ‘ mZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

24050.D NP101901.M Fri Oct 26 10:26:08 2001 Page 2 NYC-WTC_000067876

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NYC-WTC_000067876Source: NYC Law Department, mirrored locally

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