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GC/MS analysis results for sample AD23471, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23471 conducted on October 16, 2001.

NYC-WTC_000088604–000088623

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088614
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0901\23471.D Vial: 19 Acq On : 10 Oct 2001 6:53 am Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.73 0.68 ug/1 65171 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-PentanoJz< 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Hexa^r, (S)- 102 C6H14O 052019-78-0 64- 4 2-But^ol 74 C4H10O 000078-92-2 50 Abundance Scan 184 (6.733 min): 23471 .D (-) m/z 44.95 100.00% 40 J ■ asa 41 69 ' ' I ' ' ' ' I ' 535659 I 84 87 6.40 6.60 6.80 7.00 ' I" " I''" I'"' I" " I ‘ ' I "' ■ 111' ■ I " ' i''' h'"' i'"' I'" 71" I"'' I' m/z 69.00 15.60% •n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582: 2-Hexanol 4

IKHW ............ 6.40 6.60 6.80 7.00 27 m/z41.00 13.81% 69

■n/z-> 19 I'''' I'''' I A 31 57 8487 I " 11 " 11 H 1111,,. I , 1. 111 I , 111 I .. I, ,. 11111,1.,,, I, 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ^bundance #63545: 2-Pentanol. 4-methyl- 40 6.40 6.60 6.80 7.00 Sa "m/z 43705 9.35%

69

u 57 27 39 4z I I'''' I'''' I'''' I ‘ 11.1.111111111.111 I 85V ' I '■'t’tI 11' I' ‘' ' I''' 11'''' I'' ‘' I ‘' 11'''' I'' ‘' I' Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769: 2-Hexanol, (S)- ' ' I ' ' ' ' I ' 40 6.40 6.60 6.80 7.00 m/z 44.00 8.83% c

55 84 87 ' ’ I' " ‘ I' " ‘ I'' " I " '' I ‘" I " " I " ' ‘ I " " I' " ' I' ii/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

23471.D NP091101.M Thu Oct 11 13:15:25 2001 Page 4

NYC-WTC_000088614

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NYC-WTC_000088614Source: NYC Law Department, mirrored locally

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