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GC/MS analysis results for sample AD23471, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23471 conducted on October 16, 2001.

NYC-WTC_000088604–000088623

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23471.D vial: 19 Acq On : 10 Oct 2001 6:53 am Operator -. 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.51 ug/1 48469 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tenta .ve ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H14O 000623-37-0 90 2 3-Pentanol 88 C5H12O 000584-02-1 40 3 3-Pentam , 2-methyl- 102 C6H14O 000565-67-3 39 4 Amylen ydrate 88 C5H12O 000075-85-4 38 Abundance Scan 172 (6.623 min): 23471 .D (-) m/z 59.05 100.00% 5)9

c 73 lililil 43 6.20 6.40 6.60 6.80 7.00 44 >.. ........ .. ..... ■m/z 55.00 81.97% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ^bundance #63531:3-Hexanol

5000 73 I ' I ' 6.20 6.40 6.60 6.80 7.00 43 m/z 73.00 52.69% 14 I'".I-......... 11" " I" " I" " I" "I" " I" " I p ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62944: 3-Pentanol 5(9 —1111111111 I in'*! 111111 !■ I ■

6.20 6.40 6.60 6.80 7.00 5000 31 ■m/z 43.05 29.01% 41

2^ I I TTTJT . ...... . I' " ‘ I'' " I " '' I'' " I'"' I' " ' I " " I' "' I' " ' i' ‘' r n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 \bundance #63561: 3-Pentanol, 2-methyl- 5^ 6.20 6.40 6.60 6.80 7.00 “mTz 41.00 23.00%

5000 73

31 45 85 I........ I..... 4 l'".f^4-|-.r TpT-rrp-rrTpTTTyrTTTpTTTyrrT^^ 102 ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

23471.D NP091101.M Thu Oct 11 13:15:23 2001 Page 3

NYC-WTCZo6bO88613 ‘

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NYC-WTC_000088613Source: NYC Law Department, mirrored locally

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