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GC/MS analysis results for sample AD23471, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23471 conducted on October 16, 2001.

NYC-WTC_000088604–000088623

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088615
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23471.D Vial: 19 Acq On : 10 Oct 2001 6:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

11.63 0.53 ug/1 50861 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 TentativexID MW MolForm CAS# Qual

1 1,4-Dichlorobeii^e!ne-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,3z4^d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 Benzenamine.<^-methyl-4-nitro- 152 C7H8N2O2: 000099-52-5 22 4 Benzenam^jfe, 2-methyl-5-nitro- 152 C7H8N2O2! _______000099-55-8 14 4bundance / Scan 717 (11.626 min): 23471 .D (-) m/z 149.90 100.00% 1‘IO

550 115 I |Vi I i-r-r-i-i 52 78 11.20 11.40 11.60 11.80 12.00 38 45 I ,1 687 "I........ .................... . ' I ' ‘ ' I ' ' ' ' I ' .1'1............... m/z 151.90 . 53.88% Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000- 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 30.01% 35 Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 Tn/z 77795 19.71%

35 87 I I h‘r|-i I I i-p-m-j-ri ' 60 ' 70 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ n/z-> 30 40 50 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 1!i2 11.20 11.40 11.60 11.80 12.00 “inTz 52700 14.22%

5000 51 94 66 ' I ' ' ' ' I ' ' ' ' I ' Tl/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23471.D NP091101.M Thu Oct 11 13:15:28 2001 Page 5

NYC-WTC_000088615

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NYC-WTC_000088615Source: NYC Law Department, mirrored locally

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