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GCMS analysis results, sample AD25600, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25600 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069754–000069766

Folder label: “GCMS Scan X 10/27/01 An 11/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25600.D Vial: 11 Acq On : 17 Nov 2001 12:48 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.86 ug/1 178373 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tj .tative ID MW MolForm CAS# Qual 1 2-Hexanonj 100 C6H12O 000591-78-6 86 2 2-Hexani^e, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Methy: Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 Oxir< .e, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Abundance Scan 151 (6.434 min): 25600.D (-) m7z 43705 100.00% 43

58 5000

71 86 ‘>00 6.66' 6,60 6.80 U—T—4t4UX “mTz 58.05 56.02% nfe-> 20 30 40I 50 60 70 80 90 100 110 120 130 140 ^Kbundance #1556:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 Wz 5^00 15.49% 27 ' I ‘‘ .1 71 ■>“

tt/z-> 20 30 40 50 eo' ‘' '70 ‘' 80 '90' ioo iio' '126' iso 'w Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.0) 6.Z) 6.40 6.60 6.80 5000 41.05 15.44%

71 85 100 I 140 ' 1 ' ' ‘ ' I ' ' ' ' 1 I ' I'''' I' Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63351: Methyl Isobutyl Ketone 43 6.66 'e.^' 6.^ m/z 100.00 12.15% 5000 58 85 100 ■ 7?.. 1, . I,,, TiZz-> 20 30 40 TO ‘ ‘ ‘76 " " '96' ‘ 'i66"ii6' '126' '136' '140 6.00 6.20 6.40 6.60 6.80

25600.D NP103001.M Tue Nov 27 09:40:04 2001 Page 2

NYC-WTC_000069763

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NYC-WTC_000069763Source: NYC Law Department, mirrored locally

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