GC/MS analysis report for sample KD25735, Nov 2001

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Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV1601\25735.D vial: 18 Acq On : 17 Nov 2001 7:37 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C;\DATABASE\NBS75K.L ****************************************************************'***** Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.44 0.45 ug/1 99822 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexano: 100 C6H12O 000591-78-6 91 2 2-Hexan( .e, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Methyl sobutyl Ketone 100 C6H12O 000108-10-1 58 4 Oxir e, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 39 Abundance / Scan 152 (6.442 min): 25735. D (-) m/z 42.95 100.00% 43

58 5000

85 100 I. 71 6.00 6.20 6.40 6.60 6.80 I, l,.,,I| 49 I I ■m/z 58.05 57.27% Tife-> 20 30 40 50 60 70 80 90 i6o' 'i-io' w' w' '140 Abundance #63387:2-Hexanone 43

58 5000 6.00' 'sjo' 6.^ 6?^ ' 100 “iriTz SYTOO 17773% 71 • I • • ■ I I ■ • I >‘1 I , I I I '''' i ‘' I ‘' I' Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Aibunctence #11968:2-Hexanone, 4-hydroxy-3-propyl- 4(3

58 6.00 ‘ 6.^ ‘ ' 6.^ ' 6,60 T 6.80 5000 29 m/z 100.05 14.52%

tt/z-> ' I ' ‘ 20 ' I • ■ • • I I i ■ • I ■ 30 40 50 X ' ’ I ‘ 60 70 71 1,1 ,.

80 85 ii, 100 I , ,

90 100 110 , 1, 11

120 I

130 140 uo" Abundance #63350: Methyl Isobutyl Ketone 4|3 6.00 6.20 6.40 6.60 6.80 m/z 41.05 13.81% 5000

Tife~> vxx 20 30 40 1-rrp 50 58

■ eo''' 70 " ao' " 85 1. 100 .... "ioo' 'ii6" w"^"146 6.00 6.20 lU 6.40 6.60 6.80

25735.D NP103001.M Thu Nov 29 08:59:11 2001 Page 1

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