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GCMS analysis results for sample AD24950, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24950 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069128–000069138

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24950.D Vial: 18 Acq On : 7 Nov 2001 5:20 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 99767 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Te<htative ID MW MolForm CAS# Qual 1 1,4-Dichlora(benzene-d4 150 C6C12D4 003855-82-1 42 2 Benzene-1,y3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Acenaphthwene 152 C12H8 000208-96-8 9 4 Biphenylerne 152 C12H8 000259-79-0 7 Abundance 7 Scan 712 (11.577 mtn): 24950.D (-) m/z 149.90 100.00% liiO

5000- 115 52 78 1120 11.40 11.60 11.80 12.00 I . , 61 4^ m7FT;5T79^^^”6J70^ tVz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 IO) Abundance #9593:1,4-Dichlorobenzene-d4 liiO

5000 115 T t 78 1120 11.40 11.60 11.80 12.00 52 m/z 114.90 36.21% 35 T-r-p-r 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundanca #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 500) 52 78 m/z 52.00 . 15.78%

35 87 I I • I'''' I'''' I' rrt-p T I' ‘' I nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundanoe #67014: Acenaphthylene I—]—n—'>1'1 r-P]—I ‘ . I I I I I 1 I r- 1$2 11.20 11.40 11.60 11.80 12.00 m/z 77.95” 15.32% 5000-

76 98 126 ■ 1 • '"I ■ 1 • • • 11 ‘ Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 iso' 11 jo' 11'40 i?eo 'i'iTm '12.00

24950.D NP103001.M Fri Nov 16 15:31:03 2001 Page 2

NYC-WTC_000069137

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NYC-WTC_000069137Source: NYC Law Department, mirrored locally

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