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GCMS analysis results for sample AD24291, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24291 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068171–000068184

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068179
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24290.D Vial: 6 Acq On : 31 Oct 2001 9:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.70 ug/1 101027 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone^ 100 C6H12O 000591-78-6 90 2 2-HexaneJne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 3 2-He»^one, 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 74 4 OxiXane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 Scan 150 (6.424 tnin): 24290.D (-) m/z 42795 100.00% Z 43

58 5000

71 85 100 6.00 ' 6.^ 6.40 ' 6.60' ' 6,80'

nfe-> 20 UJJ k 30 40 50 60 'I.. . 70 80 90 100110lSlM140 ■m/z 58.05 55.38% Abundance #1556:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 “mTz 41.05 14.24% 27 1 71 85 ITO ■ ,7 I , I , ,1, , I I I I |l| I I I rU-T', I I I I . I I I I I I I I . I I I I I nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 57700 13.95%

' I'''' I' -t+ J. 71 I 85 ,1, 100 I.... I.... I.... I, 140 Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 10.73% 5000 I 58 27

nZz-> UM 20 30 40 50 60 ' I'l • ' ' I ■ 70 7 80 90 190 • I • ' ■ ■ I ■ ■ ' ' I ' ' ■ ' I ' ' ' ' I ■ ■ ' ' I ‘ 100 110 120 130 140 6.00 ,

6.20 . ,__, I I

6.40 r

6.60 I I I

6.80 1

24290.D NP103001.M Fri Nov 02 12:02:37 2001 Page 1

NYC-WTC_000068179

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NYC-WTC_000068179Source: NYC Law Department, mirrored locally

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