GCMS analysis results for sample AD27823, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27823.D Vial: 31 Acq On : 19 Dec 2001 8:32 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst- : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.39 0.87 ug/1 185631 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone/ 000591-78-6 91 100 C6H12O 2 2-Hexanone, 4-hydroxy-3-propyl- 062338-17-4 64 158 C9H18O2 3 2-Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O21 061141-74-0 59 4 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H120 ______ 072221-03-5 50 Abundance 7 Scan 147 (6.391 mln): 27823.D (-) " p m/z42.95100.00%

5000

miz-> Abundance 43

—... -5..L 70 80 90 100 110 120 130 140 20__ 30___ 40__ 50

43 58

60 7 85 #63384:2-Hexanone 10 _M 6.00 m/z 6.20 58.05 6.40 6.60 55.08% 6.80

.......... 5000 58 6.00 6.20 6.40 6.60 6.80 29 17.20% i 71 85 100___________________ 11 ■ ■ IT 1 —H t-m-r 60 70 80 90 100 110 120 130 ' 140 m/z-> 20 30 40 50 ) Abundance #11968; 2-Hexanone. 4-hydrovy-3- propyl- 43 58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 15.26%

71 85 100 ; I , । > । > ।। । । ■ I ■ ' ■ ' i ■ ' ' ' l ■ • ■ ■ I ‘ 140 ■ I ' ■ ■ ’ I ■ ' 1 1 I ' 1 ' ' I ' 1 1 ' I 1 1 ' 'T1"1 ' 1 1 1 ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 43 6.00 6.20 6.40 6.60 6.80 m/z 100..05 9.45% i 5000 58 27 72

m/z-> ' 1111 1 1 11 11 T 1 " I " 20 30 40 50 60 l 70 85 TIPBIT 80 90 100 100 ' i ■ ' ' ' i 1 ' ' 1 I ' 1 1 1 1 1 1 110 120 130 140 CA ----- -FPP I 6.00 6.20 6.40 6.60 6.80 I t

27823.D GCMS1126.M Wed Jan 02 12:08:05 2002 Page 2

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