GCMS analysis results for sample AD27772, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27772.D Vial: 28 Acq On : 19 Dec 2001 5:36 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst - : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.99 ug/1 321038 1,4-Dichlorobenzene-d4 11.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H1802 062338-17-4 83 3 2-He: none, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 74 4 Meth 1 Isobutyl Ketone 100 C6H120 ________ 000108-10-1 58 Abundance — Scan 148 (6.401 min): 27772.D (-) m/z 42.95 ' 100.00% 43

.58 5000

' i 1 * ■ 1 i ■ ■ 71 85 100 6.00 6.20 6.40 6.60 6.80 i? ................ TTrr i । 1। TIT +504 I 1 TTTn—uurnnotr—uunun’tuTrr m/z 58.0,5 53.01% miz-> 20__ 3040 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

5000 58 —1TITT TTmmrrrum" 6.00 6.20 6.40 6.60 6.80 m/z 57.00 15.36% 27 71 85 100 1. 1. '. —. I. ■. '. '. 6. + i-P 1 *1 p 100 i10 120 130 140 miz-? 20 30 40 50 60 70 80 90 Abundance 211268 2-Hayanone, 4-hydroxy-3-propyl- 43 58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 41.05 14.36%

71 85 100

m/z-> 20 m 30 40 50 60 70 TIP TIPPIT । 80 90 100 110 TttrT"TrIIT 120 130 140 140 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- < i < • ‘ | • » ■ ' | • • -J-T-r-r-r-j-r-r 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 9.51%

_ W 5000 58 27 72 - 85 100______________________ —1—1—I—J—--rTM*.1.1.1.. ■ p ■1 ■ ।1 TT P 11' 1 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

27772.D GCMS1126.M Wed Jan 02 12:02:24 2002 Page 2

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