GCMS analysis results for sample AD27772, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27772.D Vial: 28 Acq On : 19 Dec 2001 5:36 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst • : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.29 0.65 ug/1 212364 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Pentanone, 2-methyl- 100 C6H120 000565-69-5 43 3 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 42 4 Hexane, 2,4,4-trimethyl -_____________ 128 C9H20 ___ 016747-30-1 36 Abundance Scan 136 (6.291 min): 27772.D (-) m/z 43.05 , 100.00% 43 57

71 5000- 100 — - ।, N _ 6.00 6.20 6.40 6.60 50 .. । 85 mmmpmmmmmmllll Th HTTTTTTTTT TTTTTTTTTTT + m/ z 57.00 83.23% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63358: 3-Hexanone 43 57

5000 71 100 6.00 6.20 6.40 6.60 m/z 71.00 52.35%

U , 85 । h i j । > 111 p n 11 m n 111 i 111 n 11 TT HT Tptfuuor TTTTTTTTTTTTT TTUTII’IT miz- > 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance 363398. H-entanone, 2-methyl- 57 43 6.00 6.20 1( 6.40 ' 6.60 5000 m/z 100.0,5 30.43% 100 71 TTT—gtTTTTTT 38 , TTTTT TTTTTTTTTTT TTTTTTTTT85 i miz-> 5 10 15 20 25 JO 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62861: Butane, 2,2-dimethyl- PTm— TT 1 • TTTTT —T 43 57 6.00 6.20 6.40 6.60 71 m/z 41.05 26.81% 5000

miz-> 15 TTTTTITT 29

11,111111H mmmTTTTT ‘UITTTTTTTTTTTTTTTTTTTTTTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 VA 6.40 6.60

27772.D GCMS1126.M Wed Jan 02 12:02:19 2002 Page 1

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