GCMS analysis results for sample AD27818, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27818.D Vial: 29 Acq On : 19 Dec 2001 6:34 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.39 0.97 ug/1 294297 1,4-Dichlorobenzene-d4 11.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan .e 100 C6H120 000591-78-6 91 2 2-Hex: one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 2-H anone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 83 4 Me yl Isobutyl Ketone 100 C6H120 000108-10-1 64 Abundance 43 ■ Scan 147 (6391 min): 27818.D (-) m/z 43.05 ”100.00%

58 5000-

' 1 ' 1 85 100 6.00 6.20 6.40 6.60 6.80 -37l +50 71 i | i111 'r1 ’ ■ ■ । ■ ■' ■ p m/ z 58.0 53.30% m/z->20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384: 2-Hexanone 43

5000 58 TTITT————TTT I . 6.00 6.20 6.40 6.60 6.80 29 m/z 41.00 15.90% i miz-2 20 ' P 1 TT ■ 30 —+40 50 ‘60IT 1 " p 1 71 85 100 TIPTTPTPTTITWIPTTT 70 80 90 100 110 120 130 140 Abundance #1 1168. 2-Hexanone, 4-hydroxy-3-propyl- 43 ....... 58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 15.26%

m/z-> Abundance : ! ; . V - 140 TTDTTTTTITTTTTTPTTT 20 30 40 43 :

50 . 60__ 70_ 80 71 85 90 100 100 #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 110 120 130. 140 _W 6.00 6.20 6.40 6.60 6.80 m/z 100.05 10.05% 5000- 58 27 72 85 100 11 ■ " ' I ‘ 111 p - TTTTTTIPTTT i ) ti i । j . ... । ... . । r . miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

27818.D GCMS1126.M Wed Jan 02 12:06:10 2002 Page 2

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