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GCMS analysis results for sample AD27818, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27818 conducted on January 3, 2002.

NYC-WTC_000033641–000033652

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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Scanned page image, NYC-WTC_000033650
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27818.D Vial: 29 Acq On : 19 Dec 2001 6:34 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************** ******* ****************************** * * * * * Peak Number 3 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.53 0.45 ug/1 137702 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 74 2 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 36 3 3-Pentanol 88 C5H120 000584-02-1 33 4 Hexane, 1 -ethoxy- 130 C8H180 ____ 005756-43-4 33 Abundance Scan 162 (6.529 min): 27818.D (-) m/z 59.00 100.00% 59

5000 73 41 TTInDDuTTDTTTTTerrr 6.20 6.40 6.60 6.80 i ' ' ' • i ■ ■ ■ ■ i ' ——50— + — 86 T t TT 1. '. TT. I.. -T TPT m/z 55.00 75.47% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1762: 3-Hexanol 59 31 5000 43

■ ■ i ■ • ■ r I T- ‘ । r । I 11 > • । । । — 73

TT —PT 102 m/z 7 6.20 6.40 6.60 6.80 44.35%

miz- Abundance 10 20 30 40 50 60 70 #1781: SPentanol, 2-methyl- 80 90 100 110

59 6.20 6.40 6.60 PT ....... 6.80 5000 31 73 m/z 41.05 24.57% __ 45 15 -P — , , , T-i-j-r-r TnnmiT m/z-s 16 20 30 40 50 60 70 80 90 100 110 Abundance #62942:3-Pentanol IIP , ----- 59 6.20 6.40 6.60 6.80 m/ z 4 .00 23.53% 31 5000 41

miz-> ---2— — 10 20 30 + r. '. I TT 40 50 , T , TTTT I, ... । ,।____________ 60 70 80 < _______________ TTT 87 । । r । । । । . । i । 90 100 110 T’ICTmmu—ummLL’TTTT 6.20 6.40 6.60 6.80

27818.D GCMS1126.M Wed Jan 02 12:06:15 2002 Page 3

NYC-WTC_000033650

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NYC-WTC_000033650Source: NYC Law Department, mirrored locally

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