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GCMS analysis results for sample AD27771, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27771 conducted on January 3, 2002.

NYC-WTC_000033580–000033592

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27771.D Vial: 30 Acq On : 19 Dec 2001 7:33 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.53 0.51 ug/1 134339 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol. 102 C6H140 000623-37-0 72 2 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 38 3 2-Pro] anol, 2-methyl- 74 C4H10O 000075-65-0 36 4 2, 3-Butanediol ,2,3- dimethyl - 118 C6H14O2 000076-09-5 33 Abundance Scan 161 (6.525 min): 27771.D (-) m/z 59.0 5100.00% 59 55

5000 - 73 41 TTTtr. T. i. '. T Tprr.■. TT 6.20 6.40 6.60 6.80 -++ 447+ —67+4 miz-2____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 84 +TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT m/z 54.9, 75.81 Abundance #63531:3-Hexanol : 59

5000 73 । ' I 1 1 1 1 I ' 1 ' 1 I ' ■ ' ' i 1 r' ' i 6.20 6.40 6.60 6.80 43 m/z 73.00 44.57 i • • i" " i" " i ITT TTTTTTTTTT TTUT T‘ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561. d-Pentanol, 2-methyl- 59 TIT —TTPT TIT 6.20 6.40 6.60 6.80 5000 73 m/z 41.05 23.03? 31 __ 45 T TTTTT TTTpg 85 102 in " I T I'1111 m/z—> 20. 25 30.. 35.. 40 45 50.. 5560_ 65 70_ 75_ 80_ 85 90_ 95_100 105110 Abundance #62572: 2-Propanol, 2-methyl- TTIETTTTTTTTTTTTT 59 6.20 6.40 6.60 6.80 m/z 4 .05 20.62 5000 31 41

26 TTTTTTTTTTTTTTTTTTTT TTTD—UTTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.20 6.40 6.60 6.80

27771.D GCMS1126.M Wed Jan 02 12:01:02 2002 Page 3

NYC-WTC_000033589

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NYC-WTC_000033589Source: NYC Law Department, mirrored locally

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