GCMS analysis results for sample AD27771, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC 1901\27771.D Vial: 30 Acq On : 19 Dec 2001 7:33 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.40 1.18 ug/1 314562 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

"50 1 2-Hexanone/ 100 C6H120 000591-78-6 91 2 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H120 072221-03-5 86 3 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H1802 062338-17-4 64 4 2-He anone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 59 Abundance, ........... Scan 147 (6,397 min): 2777W (-) “ " 43

58 5000

85 100 6.00 6.20 6.40 6.60' 6.80 | +51 ................. .. miz->____ 20...... 30 ... 40 — 11 1— 11 50 80 90 100 60 71

70 j 'I 1 ' 1 1 I 1 1 •' i ■ ■' ■ i'' ■ ■ । ■ ■ ■11 ■ ■ 110 120 130 140 m/z 58.05 52.30% Abundance #1556: 2-Hexanone 43

58 TTTTTuTTTTT—TT 5000 6.00 6.20 6.40 6.60 6.80 m/z 57.00 17.51% 1 27 71 85 100 - I trrT T i ' ' ' 1 P ' ' ■ i ■ ' ' ■ i ‘ ' — 1 ' P— PPPPP — 1 . . m/z->____ 20 30___ 40 50 60 70 80 90 100 110 120 130 140 Abundance #1430: Oxirane 2-methyl-2-(1-methylethyl)- 43 58 6.00 6.20 6.40 6.60 6.80 5000 m/z 41.05 16.54%

MA 71

..... 30.... ,52 1 ‘"I"11 1 1 P ' ‘ ■ I M11 11 ’ ri p 85 100

miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 6.00__ 6.20 6.40 6.60 6.80 m/z 100.00 9.34% 58 5000 29

71 85 100 140 ■ i ■' TH TIt -PPP — TTVTDTTTT EPPTT > | « i 1 i | i > • 1 | < r' 1 ] । i miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 6,00 6.20 6.40 6.60 6.80

27771.D GCMS1126.M Wed Jan 02 12:00:57 2002 Page 2

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