GCMS analysis results for sample AD27772, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27772.D Vial: 28 Acq On : 19 Dec 2001 5:36 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************** ************************************* Peak Number 3 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.53 0.51 ug/1 166444 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol / 102 C6H140 000623-37-0 78 2 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 45 3 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 42 4 2-Hexanol, 2-methyl- ___ __ _ 116 C7H160 000625-23-0 38 Abundance Z Scan 162 (6.530 min): 27772.D (-) m/z 59. " . 00% 59

5000 73 41 TTITr 1 1 1 1 1 ' ■ 1^1 ' ' f 6.20 6.40 6.60 6.80 37 , , 53 84 101 I7” ’I HHmmt T’’ TT i IT T‘ TTTTTTTTTTTIT m/z 55.0.0 81.06% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105J10 Abundance #63531: 3-Hexanol 59

73 TTTITTITrr TITI’rrT 5000 6.20 6.40 6.60 6.80

1 43 m/ z 73.00 47.40% TTTTTTTTTTTTTTT tTHTT TH tTTugugugr m/z->___ 20 25 30 3540 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #6355; • i-Pentanol. 2-methyl- I 59 TT I 1 f PP11II 6.20 6.40 6.60 6.80 5000 73 m/z 41.05 29.43%

VA_ 31 45 I 85 102 "11" " I " " I TUIIUTUUTTTTUTTTFTTTTTTT TTTTTT TTTTTT । i rn 11 TOTTDTr q TTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62572: 2-Propanol, 2-methyl- TIT ’ ‘ ‘ ‘ I ‘ I ‘ ‘ I ' ‘ ‘ p *TT 59 6.20 6.40 6.60 6.80 m/ z 43.05 22.13%

miz—> 5000

26 TTTTTT 31

Hm TTT—mm 41

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 N 6.40 6.60 6.80

27772.D GCMS1126.M Wed Jan 02 12:02:29 2002 Page 3

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