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GCMS analysis results for sample AD27823, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27823 conducted on January 3, 2002.

NYC-WTC_000033662–000033673

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27823.D Vial: 31 Acq On : 19 Dec 2001 8:32 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title* : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.53 0.51 ug/1 108186 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 50 3 3-Pentanol 88 C5H120 000584-02-1 42 4 Amylene Hydrate 88 C5H120 000075-85-4 39 Abundance.—.................... Scan 162 (6.529 min): 27823.D (-) m/z 59.05 100.00% 55 59

5000 73 41 ■ ■ i ■ ■ r ■ । ■ ■ ■ ' । * ' TTTTr 36 . 6.20 6.40 6.60 6.80 i1 *'11" " i HHHHTIPH mil. 67+1.. . ....... m/z 55.00 82.84% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531: 3-Hexanol 59

5000 73 TIT’T । 11 । । । 111 TII 6.20 6.40 6.60 6.80 43 m/z 73.00 47.54% I' • ’ • I •"11' ” ‘ I + +... -4 1............. . l , . . . . । . . . ■ |> I > I | I■■■|TTI I|■I I 11■I I IJ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561; 3-Pentanoi. 2-methyl 59 —— —— TTPf . . . 1 6.20 6.40 6.60 6.80 5000 73 m/z 41.00 28.90%

m/z-> Abundance ■" ।"" ।"" ।1 31

r”‘I 45 111111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #62941:3-Pentanol 85 1.......... "I" TTTTTTpTrrp-rTTp-rTTpT-nTTT^^

59 102 _N_ —II

m/z <

6.20 I I I I I

6.40 4 .00 I t I I I

6.60 I I I I I

6.80 I

25.29% I I I I I

31 5000 41 87 miz-> 11' I' mA. H 1.... 11... । ■... ।.... । r ’111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 T‘ _M_ 6.20 6.40 6.60 6.80

27823.D GCMS1126.M Wed Jan 02 12:08:09 2002 Page 3

NYC-WTC_000033671

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NYC-WTC_000033671Source: NYC Law Department, mirrored locally

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