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GCMS analysis results for sample AD23996, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067767–000067781

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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Scanned page image, NYC-WTC_000067777
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23996.D Vial: 4 Acq On : 25 Oct 2001 3:37 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Paramsj LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.59 0.45 ug/1 86125 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3 -Hexanol . 102 C6H14O 000623-37-0 90 2 3-Pentanol, 2-methyl- 102 C6H14O 000565-67-3 45 3 3-Pentanol 88 C5H12O 000584-02-1 42 4 Aigylene Hydrate_____________________ 88 C5H12O 000075-85-4 38 Abundance Scan 169 (6.593 min): 23996.D (-) m/z 59.05 100.00% 59

5000 73 43

6.^ 6.40 6.60 6.80 7.00 .""i."!|lill|„„p^ 84_________ 101 TjrrTTJTTTTTTTTTpTTTJ^^^ m/z 55.00 92.49% mZz-> 20 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #63531:3-Hexanol 50

5000 73 'Vf'f-T-rTy-rT-r-T==5=r=r-r^^ 6.20 6.40 6.60 6.80 7.00 43 m/z 73.00 49.49% 4TT4ttTTTTTTr 44 t

L +t Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561:3-Pentanol. 2-methyl- 50 6.20 6.40 6.60 6.80 7.00 5000 73 m/z 42.95 33.67% A 31 45 85 I..... ^4r'"l 4 102 Tlfe-> Abundance I ‘' I"'' I I........ 'll" TpTTTpTTTTrrrrjTTTTpTTIT^^ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #62943:3-Pentanol AJ 6.y “ 6.40 " 6.60 " ‘ Abo m7z 41.05 26.10% 31 5000

41

TrpTTTp444TTpTTT44T|TTTTJTTTTf44|TTTTJTTTTpTTTpTTTyrTTTpTT-rpTrrpTTT7TTTTp^

■n/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.20 6.40 6,60 6.80 7.00

23996.D NP101901.M Fri Oct 26 10:09:42 2001 Page 3

NYC-WTC_000067777

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NYC-WTC_000067777Source: NYC Law Department, mirrored locally

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