GCMS analysis results for sample AD27823, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27823 conducted on January 3, 2002.

NYC-WTC_000033662–000033673

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27823.D Vial: 31 Acq On : 19 Dec 2001 8:32 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.64 0.57 ug/1 120958 1,4-Dichlorobenzene-d4 11.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 74 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 3 2-Hexanol, (S) - 102 C6H140 052019-78-0 64 4 2 Butanol 74 C4H10O 000078-92-2 50 Abundance Scan 174 (6.639 min): 27823.D (-) m/z 44.9.5 100.00% 45

5000

69 i 1 ’ ' 1 1 1 1 ~1 l ■ ■ ■ 1 TTT 1 1 I ' TT 41 6.20 6.40 6.60 6.80 7.00 53 58 ...................... ............... .. 1 84 87 ..........H........I" TIIWTNTITTTTTTTT m/z 69.00 16.28% miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance> 7 " #63584: 2-Hexanol 46

5000 MAMAAF 444 6.20 6.40 6.60 6.80 7.00 69 ------- m/z .41.05 --------- 14.33%

M 19 27,31 42 56 84 87 Pm] I ■ I ■ 11 ■ ■ ■ ■ .......... Hl ...... 111 ■ i ■ ■ ■ ■ i ■ ■ r ■ ■ ■ i' . i ■ ■ ■ 111 ■' ■ i ■ ■ • ■ i ■ m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #93547; 2-Pentanol, 4-methyl- 45 i ■ ' ■ ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ' ■ 6.20 6.40 6.60 6.80 7.00 5000 m/z 44.00 8.01%

27 69 38 | 42 ■I■I|H । | 57 । । I । . . TIVTIUTTITI 84 87 ■ i ■ • " i' m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769:2-Hexanol, (S) 45 6.20 6.40 ' 6.60 6.80 7.00' ' m/z .43.05 6.80% 5000

miz-> 19 I.... ..... ............ 5529 39 42. 84 87 > > । >. i. 11..।.... ।. i i ■ " ' i " ■' i ■' " i' " ' i ■" ' i ■ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69 J........ 6.20__ 6.40 6.60 6.80 7.00

27823.D GCMS1126.M Wed Jan 02 12:08:14 2002 Page 4

NYC-WTC_000033672

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NYC-WTC_000033672Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD27818, Jan 2002 · Box DEP Box 21

NYC-WTC_000033641

Laboratory report documenting GCMS analysis of environmental sample AD27818 conducted on January 3, 2002.

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