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GCMS analysis results for sample AD24291, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24291 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068171–000068184

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24290.D Vial: 6 Acq On : 31 Oct 2001 9:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.43 ug/1 62513 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H14O 000626-93-7 78 2 2-Pentan01 , 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Octa2iol, (R) - 130 C8H18O 005978-70-1 50 4 2-Ocenol 130 C8H18O 000123-96-6 39 \bundanc8 < Scan 177 (6.672 min); 24290.D (-) m/z 44795 100.00% 45 11

5000

69 6.40 6.60 6.80 7,00 T .... ,1)1,?.. I 87 I ■+l', I.... I.... II, 207 yrTTTprTTTp-rrTp m/z 69.00 16.81% T\fz-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 #63584:2-Hexanol ft 4)5

5000 6.40 6.60 6.80 7.00 69 m/z 44.05 14.42% 27 87 p+^r I I'' * • I"' ‘ I' IIII i{IIIIjll I.] .Ill I

ttZz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1773:2-Pentanol. 4-methyl- 4)5 " ' 6.M " 6.60 ' ' 6.80 7.00 5000 m/z 41.05 12.88%

n/i-> 27 1....... Ill 69 67 I 87 XJp 10 20 30 40 TO 60 70 80 90 100110120130140150160170180190 200 210 Abundance #5523:2-OclanoI. (R)- JyJ 45 6.40 6.60 6.80 7.00 m/z 42.95 11.41% 5000

•n&-> 1 o' 27 J.,.? y y ,115, ‘ 30 40' TO eb' 701^ IM 140 i'so 1 ro 170180 200210 JU 6.^' ' 6.60 ‘ ' 6.80 7.00

24290.D NP103001.M Fri Nov 02 12:02:39 2001 Page 2

NYC-WTC_000068180

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NYC-WTC_000068180Source: NYC Law Department, mirrored locally

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