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GCMS analysis results for sample AD24699, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24699 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068866–000068879

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068876
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24699.D Vial: 18 Acq On : 6 Nov 2001 4:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Hexanol, (S)- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.56 ug/1 88550 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolPorm CAS# Qual 1 2-Hex^l, (S)- 102 C6H14O 052019-78-0 78 2 2-Hexanol, (R)- 102 C6H14O 026549-24-6 78 3 2-;Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 4 Xnexanol 102 C6H14O 000626-93-7 64 ce Scan 176 (6.663 min): 24699.D (-) m/z 45.05 100.00% 4*^3

5000

•r-rr/i I I I I iVrY-p ri“

TiZz-> Abundance II 55 100 Iiii|IiH||I|I|ii l■'"'l""l 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 .X 87 >'|Hll|.ll.| m/z 6.40t 6.60 6.80 7.00 41.05 19.58% #1769:2-Hexanol. (S)- 4(5

5000 6.40 6.60 6.80 7.00 m/z 69710 14.67% 55 ? 87 TrTT7TTTT|TTTTJTTTrpTT+pTTTTTTr^ mfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1794:2-Hexanol. (R)- 4(5 _ A I A_A 6.40 6.60 6.80 7.00 5000 “mTz 43.95 13.93%

19 » , 55 ? 87 "I'" ‘ I" " I “ ‘' I' “' I “ " I “ " I ‘' "I ‘ I' ‘" 1“'' I ‘ ‘ “ mZz-> 10 15 20 25 30 35 40 45 50 60 65 70 75 80 85 90 95 100105 Abundance #63546:2-Pentanol, 4-methyI- I I . . I . , 1 I I . , . , I . . .I .r- 4(5 6.40 6.60 6.80 7.00 m7z 43.05 12.98% 5000

27 69 19 I ,1 57 I 87 I > 111111111 ■ 11111111111 ■ 111 ■ 11111 T 111111111111111 (111111111 m‘i 11111111111111111111111111111111 111

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

24699.D NP103001.M Tue Nov 13 12:08:07 2001 Page 3

NYC-WTC_000068876

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NYC-WTC_000068876Source: NYC Law Department, mirrored locally

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