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GCMS analysis results for sample AD24696, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24696 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068838–000068852

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0501\24697.D Vial: 16 Acq On : 6 Nov 2001 2:35 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.55 0.46 ug/1 75481 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hex^ol 102 C6H14O 000623-37-0 83 2 3-Heptanol 116 C7H16O 000589-82-2 38 3 3-Pentanol 88 C5H12O 000584-02-1 36 4 Ocjzanal, 7-hydroxy-3,7-dimethyl- 172 C10H20O2 000107-75-5 36 Scan 164 (6.554 min): 24697.D (-) m/z 59.05 100.00% 53

5000 73 43 6.40 6.60 6.80 ■hUs pTTTpTTTyrmrprrrr^^ 207 m/F^ 55.0.0 79.07% TiZz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance #1762:3-Hexanol 53

31 5000 43 73 T 6.20 6.40 6.60 6.80 m/z 73.00 47.86% WtTTTTyJr 102__________________________________ 1I1.HI,,,, I ,, ,, I,,,,I,, ,.I,,,,I ,,,,I , ,.,I,,,,I ,,, ,I,,, ,I,.,,I, ,, ,I,,, TiZz-> 20 30 40 50 60 70 80 90 100110120130140150 160170180190 200210 Abundance #64384:3-Heptanol 69 ■T-p-r-r-ry-r 41 620 6.40 6.60 6.80 5553 m/z 43.00 31.16% 87

98

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nfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Mjundance #62944:3-Pentanol 53 6.20 6.40 6.60 6.80 InTz 4^00 23.89% 5000 31 41

t ! " “I " ” I J... .J... IJ. I ..J Tife-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.^' 6W 6.80

24697.D NP103001.M Tue Nov 13 12:05:37 2001 Page 3

NYC-WTC_000068848

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NYC-WTC_000068848Source: NYC Law Department, mirrored locally

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