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GCMS analysis results, sample AD23948, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067675–000067689

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23947.D Vial: 14 Acq On : 18 Oct 2001 2:00 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 6.62 0.47 ug/1 44386 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexan61 102 C6H14O 000623-37-0 90 2 3-Pen^nol 88 C5H12O 000584-02-1 59 3 4-He^anol 116 C7H16O 000589-55-9 22 4 l-HeZten-4-ol 114 C7H14O 003521-91-3 10 Abundance / Scan 172 (6.618 min): 23947.D (-) m/z 59.05 100.00% 50

73 50X5 43 6.20 6.40 M 6.60 6.80 7.00 . 53 |rr,,|.r.4tllU}n,,pTtT- m/z 55.00 85.36% ■nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63531:3-H8xanoI

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z 73700 50.49% ‘' i ‘ ‘ ‘' I ‘ ‘ ‘' I' 1 ‘' I" " I"' h' I H ‘i““ +r 1" " I"" I" " I Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4bundance #851:3-Pentanol

31 6.^ " 6.^ " 6.ro ' ‘ 6,80 ‘ ' ZOO ' 5000 m/z 42.95 24.25% 41 15 2t -m-p-r .......I'll I" "I" " I"" I" " I p-rTTp-m-p Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #64378:4-Heptanol AJ A/vw, ‘ I ‘ 6.20 ' 6.40 ‘ I ‘ ‘ ‘ I 50 6.60 6.80 ZOO 73 m/z 41.05 21.62% 5CX)0 43

TTTJTT-rrpTTTTTTTTJTTTTpr^^ -ryn-TT TiZz-> 5 10 15 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 eSexoeSeloTno

23947.D NP101901.M Wed Oct 24 11:20:38 2001 Page 3

NYC-WTC_000067685

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NYC-WTC_000067685Source: NYC Law Department, mirrored locally

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