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GCMS analysis results for sample AD24219, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24219 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068037–000068054

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\NOV0101\24218.D vial: 5 Acq On : 1 Nov 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.55 ug/1 82049 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexa: 1 102 C6H14O 000626-93-7 83 2 2-Pen .nol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Bu 5.nol 74 C4H1O0 000078-92-2 50 4 2-B' anol, (R)- 74 C4H10O 014898-79-4 45 Abundance Scan 177 (6.667 min): 24218.D (-) m/z 44.95 100.00% 4)5

5000 -r. ■, , p-rr^i j 1 41 69 . 49 53 ^59 I 84 87 6.40 6.60 6.80 7.00 11111.1" 11111.. I..",. m/z 41.00 15.30% Tife-> 20 25 30 35 40 45 50 55 60 65 70 re 80 85 90 95 Abundance #63583:2-Hexanol 4)5

5000 6.40 6.OT 6W 7.00 m/ z 69.00 15.14% Ut 69 84 87 ■ 11 “ • I > > ■ > I ■ I • • 1 < I" 11 J T,fe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547:2-P8ntanol. 4-methyl- 4)5 AAA n 6.40 6,60 6,80 7,00 552 m/z 44.00 10.77%

27 69

Tife-> 20 X 25 30 35 40 ) 8487 I. I. P11.{111111... I,,, 11111111... I... 11.1I.... I,

45 50 55 60 65 70 75 80 85 90 95 Abundance #62568:2-Bulanol 45 6.40 6.60 6.80 7.00 m/z 43.05 10.49% 5000

27 31 59 56 72 -rp-n-q-r .......... Tlfe-> 2025303540 45 50556065 70 75 8085 90 95 6.40 6.60 6.80 7.00

24218.D NP103001.M Tue Nov 06 11:48:34 2001 Page 3

NYC-WTC_000068047

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NYC-WTC_000068047Source: NYC Law Department, mirrored locally

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