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GCMS analysis results for sample AD24236, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24236 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068070–000068084

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24220.D vial: 7 Acq On : 1 Nov 2001 8:52 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.42 ug/1 66670 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexary51 102 C6H14O 000626-93-7 78 2 2-Pent/nol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Oct/nol 130 C8H18O 000123-96-6 50 4 2~HeJanol, 3-methyl- 116 C7H16O 002313-65-7 39 Abundance Scan 177 (6.671 min): 24220.D (-) m/z 44.95 100.00% 4fe

5000

69 6.40I 6.60 6.80 7.00 ............ ^Jl I 87 98 m/z 42.95 16.96% mZz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63584:2-Hexanol 45

5000 JU 6.40 I ■ • • ■ I'' ■ • 1 • ■ rr 6.60 6.80 7.00 69 “mTz 41.00 16.79% 87 ■ I • I I ■ ■ ■ ■ I • ■ • • I I ■ ■ ■ I • mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63545:2-Pentanol, 4-methyi- 4|5

6.40 6.60 6.80 7.00 5000 m/z 69700 15.71%

69 I ■ ■ ■ ■ I • ■ 27 I ■ I ■ 39 , I’l I I • • I • ■ 57 I ■ I 87 ■ I ' H'i I I I ■ • I ■ • • • I I . . I I I

mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #65288:2-Octanol M I A. AA • ' • ' I ' ' ■ ' I J . . ■ I . I . . I . . , I 45 6.40 6.60 6.80 7.00 m/z 44.00 11.70% 5000

m/z-> 10 ........... 20 30 I II 40 55 ■ I ■ 'I"' I ■ 50 60 70 84 97 112 T^\--r-r-r-T-^-r-¥-r-rj-r-r-e-r-^--r-r-r-rYf-r ‘^^

70 80 90 100 110 120 6.40 6.60 L 6.80 7.00

24220.D NP103001.M Tue Nov 06 11:51:12 2001 Page 2

NYC-WTC_000068079

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NYC-WTC_000068079Source: NYC Law Department, mirrored locally

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