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GCMS analysis results for sample AD24699, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24699 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068866–000068879

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV0501\24699 .D Vial: 18 Acq On : 6 Nov 2001 4:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.54 0.43 ug/1 68598 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ■entative ID MW MolForm CAS# Qual 1 3-Hexapdl 102 C6H14O 000623-37-0 64 2 l-Hep1^^-4-ol 112 C7H12O 022127-83-9 10 3 1 -Dwpanamine, 2 -methyl- 73 C4H11N 000078-81-9 10 4 Qropane, 2,2,3-trimethyl-__________ 100 C6H12O 023120-43-6 9 W)urwfenc8 Scan 163 (6543 min): 24699.D (-) m/z 59.05 100.00%

5000 73 41 6.20 6.40 6.60 6.80 84 100 ..... 14 •|Tn.|...,l,TTT1 ra/^ 55.00 98.07% mZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #1762:3-Hexanol 5b

31 ........... 5000 43 73 6.20 6.40 6.60 6.80

,, L m/z 73.00 47.51% 102 nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #2628:1-Heptyn-4-ol

73 ........... I ■■4.,77^.......... 6.20 6.40 6.60 6.80 43 ■mTz 41.05 27.14% 5000 31

...... Ip. ra 94 l''“l ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62540:1-Propanamine, 2-niethyl- 33 _JS_a«_6S_a8o__ m/z 43705 23.69% 5000

-p+TT ' ‘ ‘ ‘ I " " 11' I' I' " ' I " " I''' ’ I " " I" " I ‘' I' I “ ‘ ‘ I' " ‘ I'" ' I'" ' 1" " I " “1" " 1' Tife-> 20 25 30 35 40 ^ 50 55 60 65 70 75 80 85 90 95 100 105 110 iso

24699.D NP103001.M Tue Nov 13 12:08:05 2001 Page 2

NYC-WTC_000068875

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NYC-WTC_000068875Source: NYC Law Department, mirrored locally

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