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GC/MS analysis report, sample AD23697, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23697 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089130–000089143

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089138
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT1501\23697.D Vial: 10 Acq On : 15 Oct 2001 8:59 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: .1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.40/ug/1 37332 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexa^ne 100 C6H12d 000589-38-8 90 2 HexanyS 3,3,4-trimethyl- 128 C9H20 016747-31-2 50 3 Butaile, 2,2-dimethyl- 86 C6H14 000075-83-2 38 4 Heptane, 3,3-dimethyl-______________ 128 C9H20 . 004032-86-4 38 <\bundance Scan 147 (6.388 min): 23697.D (-) m/z43.05 100.00% 43 57

71 5000 100

6.00 6.20 6.^ 6.60 . 6.80 85 .................. 1,11 I........l‘l........... . m/z 56795“ 89.11% TiZz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/,z 71.00 66.19%

n/z-> Abundance ................... . 10 20 30 ' - 40 43 ‘ I ' ■'' ' I '

57 50 60 71 70 _____ #51^:Hexane, 3,3,4^trimethyl- 80 90 100 110 120 A ^-.7 . ..................... 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 34.89% 27 99 ............ I ; I|, / 7 7 T,, 7 113 m/z->10 20 30 40 60 70 80 90 100 110 120 \ •............ Abundance• #732: Butane, 2,2-dimethyl- 4b517- ■ - “ _____________6~60~ ' 6'80~' 71 7n/z 41705 24.19% 29 5000

15 I ' P ' ' ' P * ' ' I ■' In— ' I ' ' ' ' I ' TiZz-> 10 20 30 40 50 60 70 80 90 100 110 120 6.00 a20 6.40 6.60 6.80

23697.D NP091101.M Tue Oct 16 15:08:42 2001 Page 1

NYC-WTC_000089138

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NYC-WTC_000089138Source: NYC Law Department, mirrored locally

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