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GC/MS analysis report, sample AD23697, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23697 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089130–000089143

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089139
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound. Report Data File : C:\HPCHEM\1\DATA\OCT1501\23697.D vial: 10 Acq On : 15 Oct 2001 8:59 pm Operator: 209 -GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.62 ug/1 58078 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qua! 1 2-Hexanone X 100 C6H12O . 000591-78-6 91 2 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 - 3 Oxiranej/2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5.50 4 2-Hexap:one, 4-hydroxy-5-methyl-3-pr 172 C10H20O2; 061141-74-0 45 Abundance / Scan 158 (6.489 min): 23697.D (-) Tm/z 43.00 100.00% 4{3

58 5000

71 85 100 6.20 6.40 6.60 6.80 7^.. ...... P m/z 58.05 58.64% Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63387:2-Hexanone 43

58 5000 —. .... .. 6,20 6.40 6.60 6,80 oc 100 ~m7z 41.00 17.01% 71 85 I" " I'" • I" " 11111111 'I'... 1'1 I"" P Tife-> 20 25 30 35 40 45 50 55 60 65 70' 75 80 85 90 95 100 105 Abundance #63350: Methyl Isobutyl Ketone 4t3 ■ ■

6,20 6.40 6.60 6,80 5000 "Wz 57.00 1677^ 58

___ 27___________ _____ 85______ 100 ...... I....... I" " r " ' I'''' I'' ‘' I'' " P ttZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance - #1530: Oxirane. 2-methyl-2-(1 ^ethylethyl)- ■ ----- ---------- --- _------------ -------------- —---------- - --- ---- --- ------- .gg---- - ---- ---------------- _ -- - 6.20 6:40' '6.60 6.80’ 2 m/z 100.05 13.26% TOY 71

30 52 I 66 85 100 ... . TlTTT.pH.Tl- tTnT.|l".i TTTp-rrr|TTTTjTTTTpTTT^^ P . I . . . I I r. , , I , , , , I , , n/i-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105' 6.20 6.40 6.60 6.80

23697.D NP091101.M Tue Oct 16 15:08:44 2001 Page 2.

NYC-WTC_000089139

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NYC-WTC_000089139Source: NYC Law Department, mirrored locally

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