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GC/MS analysis report, sample AD23697, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23697 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089130–000089143

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089140
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound -Report Data File : C:\HPCHEM\1\DATA\OCT1501\23697.D Vial: 10 Acq On : 15 Oct 2001 8:59 pm' Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T, 6.74 0.40 ug/1 37612 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 'entative ID MW MolForm CAS# Qua!

1 2-Hexano 102 C6H14O 000626-93-7 83 2 2-Penta//ol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Hexi hol, (S)- 102 C6H14O 052019-78-0 43 4 But a: , 2-ethoxy- 102 C6H14O 002679-87-0 39.. Abundance Scan 185 (6.737 min); 23697.D (-) m/z 44.95 100.00% 4h

5000

41 69 T 53^6 84 87 6.40 6.60 6.80 7.00 r''' I' ‘' I'''' I ....... .................. ..................... m/z 69.00 17.26% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 '\bundance #63584:2-Hexanol 4(5

A / p A 5000 6.40 aeo 6.80 7.00 . 69 “niTz 41.05 14.80%, 19 2731 4:^ 56 1 84®^ "I " ■ 11' " 11 ■ ■ " I 'tI I il 111111111 Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance!_______________________ #1773:2-Pentanol, 4-methyl-__ ___________ ________ 4)5

6.40 6.60 6.80 7.00 253 m/F” 43.00 10.88%

Ti/z-> Abundance 10 15 20 25 27

30 ----- _____—_____---- --------------- 4)5—__ - 35 .4:^

40 _57___

45 50 55 60 65 #1769; 2-Hexanol,-(S)- _ _ _ 111111.. 1111 ■. 11 ■ ■I.... I" 111.1.. I.. 70 75 80 _________ .34 87 - _

85 90 95

m/z44.00 C: 8.74%

5000

69 19 ......... ^42, .................................................................................. 55 8487 TT-TT-n-r TlZZ-> 16 "is "2'6 "25 30"35 "4'0 45"^"55"6'o"65"76"75 "8o"85"9o"^ 6.40 6.60 6.80 7.00

23697.D NP091101.M Tue Oct 16 15:08:46 2001 Page 3

NYC-WTC_000089140

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NYC-WTC_000089140Source: NYC Law Department, mirrored locally

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